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Comparisons of NMR spectral quality and success in crystallization demonstrate that NMR and X-ray crystallography are complementary methods for small protein structure determination.

Snyder DA, Chen Y, Denissova NG, Acton T, Aramini JM, Ciano M, Karlin R, Liu J, Manor P, Rajan PA, Rossi P, Swapna GV, Xiao R, Rost B, Hunt J, Montelione GT,
Journal of the American Chemical Society (2005) 127(47):16505-11 PublishedPSI:Phase 2  
Northeast Structural Genomics Consortium

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X-ray crystallography and NMR spectroscopy provide the only sources of experimental data from which protein structures can be analyzed at high or even atomic resolution. ...
Crystallography, X-Ray Humans Magnetic Resonance Spectroscopy Research Design Eukaryotic Cells Animals Proteomics Protein Structure, Secondary Proteins Bacterial Proteins 
49 (Last update: 04/01/2017 11:30:27am)  
HTP NMR MicroCryoProbe Screening of Protein Samples
HTP NMR MicroCryoProbe screening of protein samples
J Am Chem Soc. 2005 Nov 30;127(47):16505-11.